Photoelectrochemical Characterization of a Robust TiO2/BDD Heterojunction Electrode for Sensing Application in Aqueous Solutions
Identifieur interne : 000A71 ( Chine/Analysis ); précédent : 000A70; suivant : 000A72Photoelectrochemical Characterization of a Robust TiO2/BDD Heterojunction Electrode for Sensing Application in Aqueous Solutions
Auteurs : RBID : Pascal:10-0217273Descripteurs français
- Pascal (Inist)
- Caractérisation, Composé de métal de transition, Oxyde de titane, Composé binaire, Electrode, Solution aqueuse, Bore, Diamant, Nanoparticule, Dépôt immersion, Anatase, Rutile, Dimension particule, Film, Oxyde d'indium, Oxyde d'étain, Oxydation, Composé organique, Glucose, Potassium, Hydrogène, Régime permanent, pH, TiO2, O Ti.
- Wicri :
English descriptors
- KwdEn :
Abstract
Titanium dioxide (TiO2) and boron-doped diamond (BDD) are two of the most popular functional materials in recent years. In this work, TiO2 nanoparticles were immobilized onto the BDD electrodes by a dip-coating technique. Continuous and uniform mixed-phase (anatase and rutile) and pure-anatase TiO2/BDD electrodes were obtained after calcination processes at 700 and 450 °C, respectively. The particle sizes of both types of TiO2 film range from 20 to 30 nm. In comparison with a TiO2/indium tin oxide (ITO) electrode, the TiO2/BDD electrode demonstrates a higher photoclectrocatalytic activity toward the oxidation of organic compounds, such as glucose and potassium hydrogen phthalate. Among all the tested TiO2 electrodes, the mixed-phase TiO2/BDD electrode demonstrated the highest photoelectrocatalytic activity, which can be attributed to the formation of the p-n heterojunction between TiO2 and BDD. The electrode was subsequently used to detect a wide spectrum of organic compounds in aqueous solution using a steady-state current method. An excellent linear relationship between the steady-state photocurrents and equivalent organic concentrations was attained. The steady-state oxidation photocurrents of the mixed-phase TiO2/BDD electrode were insensitive to pH in the range of pH 2-10. Furthermore, the electrodes exhibited excellent robustness under strong acidic conditions that the TiO2/ITO electrodes cannot stand. These characteristics bestow the mixed-phaseTiO2/BDD electrode to be a versatile material for the sensing of organic compounds.
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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en" level="a">Photoelectrochemical Characterization of a Robust TiO<sub>2</sub>/BDD Heterojunction Electrode for Sensing Application in Aqueous Solutions</title><author><name>YANHE HAN</name><affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Griffith School of Environment Gold Coast Campus, Griffith University QLD 4222</s1><s3>AUS</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ></inist:fA14><country>Australie</country><wicri:noRegion>Griffith School of Environment Gold Coast Campus, Griffith University QLD 4222</wicri:noRegion></affiliation><affiliation wicri:level="1"><inist:fA14 i1="02"><s1>School of Life Science, Liaoning Normal University</s1><s2>Dalian 116029</s2><s3>CHN</s3><sZ>1 aut.</sZ></inist:fA14><country>République populaire de Chine</country><wicri:noRegion>Dalian 116029</wicri:noRegion></affiliation></author><author><name>SHANQING ZHANG</name><affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Griffith School of Environment Gold Coast Campus, Griffith University QLD 4222</s1><s3>AUS</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ></inist:fA14><country>Australie</country><wicri:noRegion>Griffith School of Environment Gold Coast Campus, Griffith University QLD 4222</wicri:noRegion></affiliation></author><author><name>HUIJUN ZHAO</name><affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Griffith School of Environment Gold Coast Campus, Griffith University QLD 4222</s1><s3>AUS</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ></inist:fA14><country>Australie</country><wicri:noRegion>Griffith School of Environment Gold Coast Campus, Griffith University QLD 4222</wicri:noRegion></affiliation></author><author><name>WILLIAM WEN</name><affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Griffith School of Environment Gold Coast Campus, Griffith University QLD 4222</s1><s3>AUS</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ></inist:fA14><country>Australie</country><wicri:noRegion>Griffith School of Environment Gold Coast Campus, Griffith University QLD 4222</wicri:noRegion></affiliation></author><author><name>HAIMIN ZHANG</name><affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Griffith School of Environment Gold Coast Campus, Griffith University QLD 4222</s1><s3>AUS</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ></inist:fA14><country>Australie</country><wicri:noRegion>Griffith School of Environment Gold Coast Campus, Griffith University QLD 4222</wicri:noRegion></affiliation></author><author><name>HONGJUAN WANG</name><affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Griffith School of Environment Gold Coast Campus, Griffith University QLD 4222</s1><s3>AUS</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ></inist:fA14><country>Australie</country><wicri:noRegion>Griffith School of Environment Gold Coast Campus, Griffith University QLD 4222</wicri:noRegion></affiliation><affiliation wicri:level="1"><inist:fA14 i1="03"><s1>School of Chemistry and Chemical Engineering, South China University of Technology</s1><s2>Guangzhou 510640</s2><s3>CHN</s3><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>République populaire de Chine</country><wicri:noRegion>Guangzhou 510640</wicri:noRegion></affiliation></author><author><name>FENG PENG</name><affiliation wicri:level="1"><inist:fA14 i1="03"><s1>School of Chemistry and Chemical Engineering, South China University of Technology</s1><s2>Guangzhou 510640</s2><s3>CHN</s3><sZ>6 aut.</sZ><sZ>7 aut.</sZ></inist:fA14><country>République populaire de Chine</country><wicri:noRegion>Guangzhou 510640</wicri:noRegion></affiliation></author></titleStmt><publicationStmt><idno type="inist">10-0217273</idno><date when="2010">2010</date><idno type="stanalyst">PASCAL 10-0217273 INIST</idno><idno type="RBID">Pascal:10-0217273</idno><idno type="wicri:Area/Main/Corpus">004609</idno><idno type="wicri:Area/Main/Repository">003B17</idno><idno type="wicri:Area/Chine/Extraction">000A71</idno></publicationStmt><seriesStmt><idno type="ISSN">0743-7463</idno><title level="j" type="abbreviated">Langmuir</title><title level="j" type="main">Langmuir</title></seriesStmt></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Anatase</term><term>Aqueous solution</term><term>Binary compound</term><term>Boron</term><term>Characterization</term><term>Diamond</term><term>Dip coating</term><term>Electrodes</term><term>Film</term><term>Glucose</term><term>Hydrogen</term><term>Indium oxide</term><term>Nanoparticle</term><term>Organic compounds</term><term>Oxidation</term><term>Particle size</term><term>Potassium</term><term>Rutile</term><term>Steady state</term><term>Tin oxide</term><term>Titanium oxide</term><term>Transition element compounds</term><term>pH</term></keywords><keywords scheme="Pascal" xml:lang="fr"><term>Caractérisation</term><term>Composé de métal de transition</term><term>Oxyde de titane</term><term>Composé binaire</term><term>Electrode</term><term>Solution aqueuse</term><term>Bore</term><term>Diamant</term><term>Nanoparticule</term><term>Dépôt immersion</term><term>Anatase</term><term>Rutile</term><term>Dimension particule</term><term>Film</term><term>Oxyde d'indium</term><term>Oxyde d'étain</term><term>Oxydation</term><term>Composé organique</term><term>Glucose</term><term>Potassium</term><term>Hydrogène</term><term>Régime permanent</term><term>pH</term><term>TiO2</term><term>O Ti</term></keywords><keywords scheme="Wicri" type="concept" xml:lang="fr"><term>Glucose</term><term>Potassium</term><term>Hydrogène</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Titanium dioxide (TiO<sub>2</sub>) and boron-doped diamond (BDD) are two of the most popular functional materials in recent years. In this work, TiO<sub>2</sub> nanoparticles were immobilized onto the BDD electrodes by a dip-coating technique. Continuous and uniform mixed-phase (anatase and rutile) and pure-anatase TiO<sub>2</sub>/BDD electrodes were obtained after calcination processes at 700 and 450 °C, respectively. The particle sizes of both types of TiO<sub>2</sub> film range from 20 to 30 nm. In comparison with a TiO<sub>2</sub>/indium tin oxide (ITO) electrode, the TiO<sub>2</sub>/BDD electrode demonstrates a higher photoclectrocatalytic activity toward the oxidation of organic compounds, such as glucose and potassium hydrogen phthalate. Among all the tested TiO<sub>2</sub> electrodes, the mixed-phase TiO<sub>2</sub>/BDD electrode demonstrated the highest photoelectrocatalytic activity, which can be attributed to the formation of the p-n heterojunction between TiO<sub>2</sub> and BDD. The electrode was subsequently used to detect a wide spectrum of organic compounds in aqueous solution using a steady-state current method. An excellent linear relationship between the steady-state photocurrents and equivalent organic concentrations was attained. The steady-state oxidation photocurrents of the mixed-phase TiO<sub>2</sub>/BDD electrode were insensitive to pH in the range of pH 2-10. Furthermore, the electrodes exhibited excellent robustness under strong acidic conditions that the TiO<sub>2</sub>/ITO electrodes cannot stand. These characteristics bestow the mixed-phaseTiO<sub>2</sub>/BDD electrode to be a versatile material for the sensing of organic compounds.</div></front></TEI><inist><standard h6="B"><pA><fA01 i1="01" i2="1"><s0>0743-7463</s0></fA01><fA02 i1="01"><s0>LANGD5</s0></fA02><fA03 i2="1"><s0>Langmuir</s0></fA03><fA05><s2>26</s2></fA05><fA06><s2>8</s2></fA06><fA08 i1="01" i2="1" l="ENG"><s1>Photoelectrochemical Characterization of a Robust TiO<sub>2</sub>/BDD Heterojunction Electrode for Sensing Application in Aqueous Solutions</s1></fA08><fA11 i1="01" i2="1"><s1>YANHE HAN</s1></fA11><fA11 i1="02" i2="1"><s1>SHANQING ZHANG</s1></fA11><fA11 i1="03" i2="1"><s1>HUIJUN ZHAO</s1></fA11><fA11 i1="04" i2="1"><s1>WILLIAM WEN</s1></fA11><fA11 i1="05" i2="1"><s1>HAIMIN ZHANG</s1></fA11><fA11 i1="06" i2="1"><s1>HONGJUAN WANG</s1></fA11><fA11 i1="07" i2="1"><s1>FENG PENG</s1></fA11><fA14 i1="01"><s1>Griffith School of Environment Gold Coast Campus, Griffith University QLD 4222</s1><s3>AUS</s3><sZ>1 aut.</sZ><sZ>2 aut.</sZ><sZ>3 aut.</sZ><sZ>4 aut.</sZ><sZ>5 aut.</sZ><sZ>6 aut.</sZ></fA14><fA14 i1="02"><s1>School of Life Science, Liaoning Normal University</s1><s2>Dalian 116029</s2><s3>CHN</s3><sZ>1 aut.</sZ></fA14><fA14 i1="03"><s1>School of Chemistry and Chemical Engineering, South China University of Technology</s1><s2>Guangzhou 510640</s2><s3>CHN</s3><sZ>6 aut.</sZ><sZ>7 aut.</sZ></fA14><fA20><s1>6033-6040</s1></fA20><fA21><s1>2010</s1></fA21><fA23 i1="01"><s0>ENG</s0></fA23><fA43 i1="01"><s1>INIST</s1><s2>20642</s2><s5>354000180601040990</s5></fA43><fA44><s0>0000</s0><s1>© 2010 INIST-CNRS. All rights reserved.</s1></fA44><fA47 i1="01" i2="1"><s0>10-0217273</s0></fA47><fA60><s1>P</s1></fA60><fA61><s0>A</s0></fA61><fA64 i1="01" i2="1"><s0>Langmuir</s0></fA64><fA66 i1="01"><s0>USA</s0></fA66><fA99><s0>ref. et notes dissem.</s0></fA99><fC01 i1="01" l="ENG"><s0>Titanium dioxide (TiO<sub>2</sub>) and boron-doped diamond (BDD) are two of the most popular functional materials in recent years. In this work, TiO<sub>2</sub> nanoparticles were immobilized onto the BDD electrodes by a dip-coating technique. Continuous and uniform mixed-phase (anatase and rutile) and pure-anatase TiO<sub>2</sub>/BDD electrodes were obtained after calcination processes at 700 and 450 °C, respectively. The particle sizes of both types of TiO<sub>2</sub> film range from 20 to 30 nm. In comparison with a TiO<sub>2</sub>/indium tin oxide (ITO) electrode, the TiO<sub>2</sub>/BDD electrode demonstrates a higher photoclectrocatalytic activity toward the oxidation of organic compounds, such as glucose and potassium hydrogen phthalate. Among all the tested TiO<sub>2</sub> electrodes, the mixed-phase TiO<sub>2</sub>/BDD electrode demonstrated the highest photoelectrocatalytic activity, which can be attributed to the formation of the p-n heterojunction between TiO<sub>2</sub> and BDD. The electrode was subsequently used to detect a wide spectrum of organic compounds in aqueous solution using a steady-state current method. An excellent linear relationship between the steady-state photocurrents and equivalent organic concentrations was attained. The steady-state oxidation photocurrents of the mixed-phase TiO<sub>2</sub>/BDD electrode were insensitive to pH in the range of pH 2-10. Furthermore, the electrodes exhibited excellent robustness under strong acidic conditions that the TiO<sub>2</sub>/ITO electrodes cannot stand. These characteristics bestow the mixed-phaseTiO<sub>2</sub>/BDD electrode to be a versatile material for the sensing of organic compounds.</s0></fC01><fC02 i1="01" i2="X"><s0>001C01I</s0></fC02><fC02 i1="02" i2="X"><s0>001C01J</s0></fC02><fC02 i1="03" i2="X"><s0>001C01J02</s0></fC02><fC03 i1="01" i2="X" l="FRE"><s0>Caractérisation</s0><s5>01</s5></fC03><fC03 i1="01" i2="X" l="ENG"><s0>Characterization</s0><s5>01</s5></fC03><fC03 i1="01" i2="X" l="SPA"><s0>Caracterización</s0><s5>01</s5></fC03><fC03 i1="02" i2="3" l="FRE"><s0>Composé de métal de transition</s0><s5>02</s5></fC03><fC03 i1="02" i2="3" l="ENG"><s0>Transition element compounds</s0><s5>02</s5></fC03><fC03 i1="03" i2="X" l="FRE"><s0>Oxyde de titane</s0><s5>03</s5></fC03><fC03 i1="03" i2="X" l="ENG"><s0>Titanium oxide</s0><s5>03</s5></fC03><fC03 i1="03" i2="X" l="SPA"><s0>Titanio óxido</s0><s5>03</s5></fC03><fC03 i1="04" i2="X" l="FRE"><s0>Composé binaire</s0><s5>04</s5></fC03><fC03 i1="04" i2="X" l="ENG"><s0>Binary compound</s0><s5>04</s5></fC03><fC03 i1="04" i2="X" l="SPA"><s0>Compuesto binario</s0><s5>04</s5></fC03><fC03 i1="05" i2="X" l="FRE"><s0>Electrode</s0><s5>05</s5></fC03><fC03 i1="05" i2="X" l="ENG"><s0>Electrodes</s0><s5>05</s5></fC03><fC03 i1="05" i2="X" l="SPA"><s0>Electrodo</s0><s5>05</s5></fC03><fC03 i1="06" i2="X" l="FRE"><s0>Solution aqueuse</s0><s5>06</s5></fC03><fC03 i1="06" i2="X" l="ENG"><s0>Aqueous solution</s0><s5>06</s5></fC03><fC03 i1="06" i2="X" l="SPA"><s0>Solución acuosa</s0><s5>06</s5></fC03><fC03 i1="07" i2="X" l="FRE"><s0>Bore</s0><s2>NC</s2><s5>08</s5></fC03><fC03 i1="07" i2="X" l="ENG"><s0>Boron</s0><s2>NC</s2><s5>08</s5></fC03><fC03 i1="07" i2="X" l="SPA"><s0>Boro</s0><s2>NC</s2><s5>08</s5></fC03><fC03 i1="08" i2="X" l="FRE"><s0>Diamant</s0><s5>09</s5></fC03><fC03 i1="08" i2="X" l="ENG"><s0>Diamond</s0><s5>09</s5></fC03><fC03 i1="08" i2="X" l="SPA"><s0>Diamante</s0><s5>09</s5></fC03><fC03 i1="09" i2="X" l="FRE"><s0>Nanoparticule</s0><s5>10</s5></fC03><fC03 i1="09" i2="X" l="ENG"><s0>Nanoparticle</s0><s5>10</s5></fC03><fC03 i1="09" i2="X" l="SPA"><s0>Nanopartícula</s0><s5>10</s5></fC03><fC03 i1="10" i2="X" l="FRE"><s0>Dépôt immersion</s0><s5>11</s5></fC03><fC03 i1="10" i2="X" l="ENG"><s0>Dip coating</s0><s5>11</s5></fC03><fC03 i1="10" i2="X" l="SPA"><s0>Depósito inmersión</s0><s5>11</s5></fC03><fC03 i1="11" i2="X" l="FRE"><s0>Anatase</s0><s5>12</s5></fC03><fC03 i1="11" i2="X" l="ENG"><s0>Anatase</s0><s5>12</s5></fC03><fC03 i1="11" i2="X" l="SPA"><s0>Anatasa</s0><s5>12</s5></fC03><fC03 i1="12" i2="X" l="FRE"><s0>Rutile</s0><s5>13</s5></fC03><fC03 i1="12" i2="X" l="ENG"><s0>Rutile</s0><s5>13</s5></fC03><fC03 i1="12" i2="X" l="SPA"><s0>Rutilo</s0><s5>13</s5></fC03><fC03 i1="13" i2="X" l="FRE"><s0>Dimension particule</s0><s5>14</s5></fC03><fC03 i1="13" i2="X" l="ENG"><s0>Particle size</s0><s5>14</s5></fC03><fC03 i1="13" i2="X" l="SPA"><s0>Dimensión partícula</s0><s5>14</s5></fC03><fC03 i1="14" i2="X" l="FRE"><s0>Film</s0><s5>15</s5></fC03><fC03 i1="14" i2="X" l="ENG"><s0>Film</s0><s5>15</s5></fC03><fC03 i1="14" i2="X" l="SPA"><s0>Película</s0><s5>15</s5></fC03><fC03 i1="15" i2="X" l="FRE"><s0>Oxyde d'indium</s0><s5>16</s5></fC03><fC03 i1="15" i2="X" l="ENG"><s0>Indium oxide</s0><s5>16</s5></fC03><fC03 i1="15" i2="X" l="SPA"><s0>Indio óxido</s0><s5>16</s5></fC03><fC03 i1="16" i2="X" l="FRE"><s0>Oxyde d'étain</s0><s5>17</s5></fC03><fC03 i1="16" i2="X" l="ENG"><s0>Tin oxide</s0><s5>17</s5></fC03><fC03 i1="16" i2="X" l="SPA"><s0>Estaño óxido</s0><s5>17</s5></fC03><fC03 i1="17" i2="X" l="FRE"><s0>Oxydation</s0><s5>18</s5></fC03><fC03 i1="17" i2="X" l="ENG"><s0>Oxidation</s0><s5>18</s5></fC03><fC03 i1="17" i2="X" l="SPA"><s0>Oxidación</s0><s5>18</s5></fC03><fC03 i1="18" i2="X" l="FRE"><s0>Composé organique</s0><s2>NA</s2><s5>19</s5></fC03><fC03 i1="18" i2="X" l="ENG"><s0>Organic compounds</s0><s2>NA</s2><s5>19</s5></fC03><fC03 i1="18" i2="X" l="SPA"><s0>Compuesto orgánico</s0><s2>NA</s2><s5>19</s5></fC03><fC03 i1="19" i2="X" l="FRE"><s0>Glucose</s0><s2>NK</s2><s5>20</s5></fC03><fC03 i1="19" i2="X" l="ENG"><s0>Glucose</s0><s2>NK</s2><s5>20</s5></fC03><fC03 i1="19" i2="X" l="SPA"><s0>Glucosa</s0><s2>NK</s2><s5>20</s5></fC03><fC03 i1="20" i2="X" l="FRE"><s0>Potassium</s0><s2>NC</s2><s2>FR</s2><s5>21</s5></fC03><fC03 i1="20" i2="X" l="ENG"><s0>Potassium</s0><s2>NC</s2><s2>FR</s2><s5>21</s5></fC03><fC03 i1="20" i2="X" l="SPA"><s0>Potasio</s0><s2>NC</s2><s2>FR</s2><s5>21</s5></fC03><fC03 i1="21" i2="X" l="FRE"><s0>Hydrogène</s0><s2>NC</s2><s5>22</s5></fC03><fC03 i1="21" i2="X" l="ENG"><s0>Hydrogen</s0><s2>NC</s2><s5>22</s5></fC03><fC03 i1="21" i2="X" l="SPA"><s0>Hidrógeno</s0><s2>NC</s2><s5>22</s5></fC03><fC03 i1="22" i2="X" l="FRE"><s0>Régime permanent</s0><s5>23</s5></fC03><fC03 i1="22" i2="X" l="ENG"><s0>Steady state</s0><s5>23</s5></fC03><fC03 i1="22" i2="X" l="SPA"><s0>Régimen permanente</s0><s5>23</s5></fC03><fC03 i1="23" i2="X" l="FRE"><s0>pH</s0><s5>24</s5></fC03><fC03 i1="23" i2="X" l="ENG"><s0>pH</s0><s5>24</s5></fC03><fC03 i1="23" i2="X" l="SPA"><s0>pH</s0><s5>24</s5></fC03><fC03 i1="24" i2="X" l="FRE"><s0>TiO2</s0><s4>INC</s4><s5>32</s5></fC03><fC03 i1="25" i2="X" l="FRE"><s0>O Ti</s0><s4>INC</s4><s5>33</s5></fC03><fN21><s1>144</s1></fN21><fN44 i1="01"><s1>OTO</s1></fN44><fN82><s1>OTO</s1></fN82></pA></standard></inist></record>Pour manipuler ce document sous Unix (Dilib)
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